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Standard operating procedure for soil total nitrogen - Dumas dry combustion method










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    Standard operating procedure for soil total carbon - Dumas dry combustion method 2020
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    GLOSOLAN is a Global Soil Laboratory Network which aims to harmonize soil analysis methods and data so that soil information is comparable and interpretable across laboratories, countries and regions. Evidence-based decisions are critical to the achievement of Sustainable Soil Management (SSM), food security and nutrition, and Agenda 2030 for Sustainable Development. While the quantity and quality of soil data are fundamental, soil information must also be harmonized and globally consistent to have impact. Standard operating procedures (SOPs) are sets of step-by-step written instructions that help lab staff to carry out routine operations by describing, in detail, how to perform a laboratory process or experiment safely and effectively. SOPs aim to achieve efficiency, quality of output and uniformity of performance while reducing miscommunication and failure to comply with laboratory and international standards. The harmonization of laboratory standard operating procedures and methods is at the basis of harmonizing soil laboratory data.
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    Standard operating procedure for soil nitrogen - Kjeldahl method 2021
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    This standard operating procedure (SOP) describes, in general terms, the quantification of the Kjeldahl nitrogen(KjN) content in soil samples. The advantages of this method are based on its robustness, low initial cost of the equipment and extensive application. However, there are disadvantages in using this method compared to others, for example, the use of potentially hazardous reagents that require consideration for safe operation are utilized, alongside the generation of hazardous waste and on-going cost of consumables, which can be mitigated via modified protocols that use lower quantities of reagents. Another limitation of this method is that it measures organic N and mineral N in the form of ammonium cation (NH4+), therefore, to measure the total N, the mineral N in the form of NO3- must be measured separately
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    Standard operating procedure for soil available phosphorus - Olsen method 2021
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    This procedure is suitable for calcareous, alkaline, neutral, and slightly acidic soils containing CaPO4, since the calcium concentration in the solution is suppressed by the precipitation of CaCO3, increasing PO4 concentration in solution. Neutral and slightly acid soils (pH 6.0 to 7.0) may contain both Ca- and Al-phosphates. The NaHCO3 extractant can remove Ca-phosphates and phosphate adsorbed on the surface of calcium and magnesium carbonates along with Al-phosphates and is considered the most suitable extractant for these soils.

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